TA Instruments

AR1769-0001f

28/03/2013 09:56:11

Sample name	DI 40 mm AL P100B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1769
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 09:56:11

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	6.008	-32.064	10000	20.0	5.894	31.008	-2.552	12.02	-0.2123	9381	5.3739	64.97	10.748	1074.8	3.411E-3	0.0	0.5
2.0000	9.809	12.736	10000	20.0	5.890	32.000	1.013	19.62	0.05166	9374	13.1914	24.36	26.383	2638.3	3.411E-3	0.0	0.5
3.0000	15.47	24.632	10000	20.0	5.890	33.000	1.960	30.94	0.06335	9374	26.8852	9.791	53.770	5377.0	3.411E-3	0.1	0.6
3.9960	18.42	32.364	10000	20.0	5.892	33.996	2.575	36.83	0.06993	9377	40.9568	6.913	81.914	8191.4	3.411E-3	0.1	0.6
4.9960	24.66	50.885	10000	20.0	5.890	34.996	4.049	49.32	0.08211	9374	67.5168	3.854	135.03	13503	3.411E-3	0.1	0.6
6.0000	31.58	76.621	10000	20.0	5.888	36.000	6.097	63.15	0.09655	9372	106.6360	2.350	213.27	21327	3.411E-3	0.1	0.6
7.0000	34.02	86.527	10000	20.0	5.883	37.000	6.886	68.04	0.1012	9363	126.2730	2.023	252.55	25255	3.412E-3	0.1	0.6
7.9960	39.30	108.84	10000	20.0	5.883	37.996	8.661	78.60	0.1102	9363	165.2170	1.516	330.43	33043	3.411E-3	0.1	0.6
9.0000	46.03	140.81	10000	20.0	5.875	39.000	11.21	92.06	0.1217	9351	223.1620	1.103	446.32	44632	3.411E-3	0.2	0.7
9.9960	50.95	166.97	10000	20.0	5.869	39.996	13.29	101.9	0.1304	9341	274.7430	0.8995	549.49	54949	3.411E-3	0.2	0.7
11.000	55.72	194.85	10000	20.0	5.865	41.000	15.51	111.4	0.1391	9335	326.0450	0.7517	652.09	65209	3.411E-3	0.2	0.7
12.000	60.09	221.18	10000	20.0	5.859	42.000	17.60	120.2	0.1464	9326	377.7990	0.6456	755.60	75560	3.411E-3	0.2	0.7
12.996	64.40	250.07	10000	20.0	5.853	42.996	19.90	128.8	0.1545	9315	434.6880	0.5615	869.38	86938	3.411E-3	0.2	0.7
14.000	69.14	280.33	10000	20.0	5.843	44.000	22.31	138.3	0.1613	9299	498.5770	0.4863	997.15	99716	3.411E-3	0.2	0.7
14.996	75.68	328.78	10000	20.0	5.835	44.996	26.16	151.4	0.1729	9286	594.0870	0.4053	1188.2	1.1882E5	3.411E-3	0.2	0.7
15.996	79.92	362.88	10000	20.0	5.830	45.996	28.88	159.8	0.1807	9279	665.4880	0.3632	1331.0	1.3310E5	3.411E-3	0.3	0.8
16.996	84.52	400.94	10000	20.0	5.820	46.996	31.91	169.0	0.1887	9262	740.5080	0.3241	1481.0	1.4810E5	3.411E-3	0.3	0.8
18.000	90.97	459.18	10000	20.0	5.807	48.000	36.54	181.9	0.2008	9241	854.8920	0.2792	1709.8	1.7098E5	3.411E-3	0.3	0.8
19.000	95.03	499.53	10000	20.0	5.794	49.000	39.75	190.1	0.2092	9221	931.0930	0.2553	1862.2	1.8622E5	3.411E-3	0.3	0.8
20.004	99.39	541.29	10000	20.0	5.786	50.004	43.07	198.8	0.2167	9209	1019.9900	0.2331	2040.0	2.0400E5	3.411E-3	0.3	0.8
20.996	105.8	611.84	10000	20.0	5.769	50.996	48.69	211.7	0.2300	9182	1153.2400	0.2050	2306.5	2.3065E5	3.411E-3	0.3	0.8
22.000	109.9	660.48	10000	20.0	5.753	52.000	52.56	219.8	0.2392	9156	1241.9700	0.1896	2483.9	2.4839E5	3.411E-3	0.4	0.9
22.996	114.2	710.81	10000	20.0	5.744	52.996	56.56	228.5	0.2476	9141	1344.4700	0.1751	2688.9	2.6889E5	3.411E-3	0.4	0.9
24.004	120.6	793.49	10000	20.0	5.719	54.004	63.14	241.3	0.2617	9103	1495.5000	0.1564	2991.0	2.9910E5	3.411E-3	0.4	0.9
24.996	124.7	837.60	10000	20.0	5.703	54.996	66.65	249.5	0.2672	9077	1597.7100	0.1459	3195.4	3.1954E5	3.411E-3	0.4	0.9
25.996	129.0	903.27	10000	20.0	5.681	55.996	71.88	258.1	0.2785	9042	1710.8900	0.1357	3421.8	3.4218E5	3.411E-3	0.4	0.9
26.996	135.4	993.95	10000	20.0	5.660	56.996	79.10	270.9	0.2920	9008	1881.7600	0.1228	3763.5	3.7635E5	3.411E-3	0.4	0.9
27.996	139.5	1044.7	10000	20.0	5.635	57.996	83.13	279.1	0.2979	8969	1995.6500	0.1151	3991.3	3.9913E5	3.411E-3	0.5	1.0
29.000	143.6	1114.2	10000	20.0	5.612	59.000	88.67	287.3	0.3086	8931	2115.8401	0.1082	4231.7	4.2317E5	3.411E-3	0.5	1.0
30.000	150.0	1205.5	10000	20.0	5.584	60.000	95.93	300.1	0.3197	8887	2305.6201	0.09871	4611.2	4.6112E5	3.411E-3	0.5	1.0
31.000	154.2	1264.0	10000	20.0	5.568	61.000	100.6	308.3	0.3263	8862	2432.1399	0.09323	4864.3	4.8643E5	3.411E-3	0.5	1.0
32.000	158.3	1339.0	10000	20.0	5.551	62.000	106.6	316.5	0.3367	8835	2564.8701	0.08820	5129.7	5.1297E5	3.411E-3	0.5	1.0
32.996	164.6	1439.2	10000	20.0	5.509	62.996	114.5	329.3	0.3478	8767	2773.4700	0.08085	5546.9	5.5469E5	3.411E-3	0.5	1.0
33.996	168.8	1517.3	10000	20.0	5.475	63.996	120.7	337.6	0.3577	8714	2912.5901	0.07647	5825.2	5.8252E5	3.411E-3	0.6	1.1
34.996	174.9	1621.8	10000	20.0	5.455	64.996	129.1	349.7	0.3690	8681	3127.4600	0.07098	6254.9	6.2549E5	3.411E-3	0.6	1.1
35.996	179.1	1705.8	10000	20.0	5.429	65.996	135.7	358.2	0.3789	8640	3279.7100	0.06733	6559.4	6.5594E5	3.411E-3	0.6	1.1
36.996	183.3	1765.9	10000	20.0	5.382	66.996	140.5	366.5	0.3834	8566	3507.5701	0.06376	7015.1	7.0151E5	3.411E-3	0.6	1.1
37.996	189.3	1887.6	10000	20.0	5.353	67.996	150.2	378.6	0.3968	8520	3657.8101	0.05945	7315.6	7.3156E5	3.411E-3	0.6	1.1
38.992	193.5	1980.4	10000	20.0	5.348	68.992	157.6	386.9	0.4073	8511	3822.2400	0.05686	7644.5	7.6445E5	3.411E-3	0.6	1.1
39.996	199.7	2090.5	10000	20.0	5.285	69.996	166.4	399.3	0.4166	8411	4068.1799	0.05275	8136.4	8.1364E5	3.411E-3	0.7	1.2
41.000	203.7	2173.3	10000	20.0	5.256	71.000	172.9	407.4	0.4245	8365	4232.5098	0.05041	8465.0	8.4650E5	3.411E-3	0.7	1.2
41.996	207.9	2247.1	10000	20.0	5.233	71.996	178.8	415.7	0.4301	8329	4410.8398	0.04819	8821.7	8.8217E5	3.411E-3	0.7	1.2
42.996	214.1	2390.9	10000	20.0	5.176	72.996	190.3	428.1	0.4444	8238	4675.1401	0.04494	9350.3	9.3503E5	3.411E-3	0.7	1.2
44.000	218.1	2489.8	10000	20.0	5.161	74.000	198.1	436.3	0.4542	8214	4851.1001	0.04316	9702.2	9.7022E5	3.411E-3	0.7	1.2
44.996	224.3	2609.5	10000	20.0	5.100	74.996	207.7	448.5	0.4630	8117	5129.6299	0.04035	10259	1.0259E6	3.411E-3	0.7	1.2
45.996	228.4	2701.8	10000	20.0	5.075	75.996	215.0	456.8	0.4707	8077	5318.0000	0.03871	10636	1.0636E6	3.411E-3	0.8	1.3
46.996	234.5	2814.3	10000	20.0	5.024	76.996	224.0	468.9	0.4776	7995	5601.8999	0.03636	11204	1.1204E6	3.411E-3	0.8	1.3
47.996	238.5	2936.8	10000	20.0	4.987	77.996	233.7	477.0	0.4900	7937	5797.3398	0.03489	11595	1.1595E6	3.411E-3	0.8	1.3
48.996	242.7	3025.6	10000	20.0	4.980	78.996	240.8	485.3	0.4961	7926	5999.4199	0.03365	11999	1.1999E6	3.411E-3	0.8	1.3
49.996	248.8	3142.3	10000	20.0	4.898	79.996	250.1	497.6	0.5026	7795	6302.1201	0.03149	12604	1.2604E6	3.411E-3	0.8	1.3
50.996	252.8	3266.7	10000	20.0	4.875	80.996	260.0	505.6	0.5141	7758	6510.2002	0.03035	13020	1.3020E6	3.411E-3	0.8	1.3
51.996	259.0	3409.3	10000	20.0	4.823	81.996	271.3	518.1	0.5237	7676	6831.7500	0.02860	13664	1.3664E6	3.411E-3	0.9	1.4
52.996	263.1	3504.6	10000	20.0	4.753	82.996	278.9	526.2	0.5300	7564	7047.1499	0.02732	14094	1.4094E6	3.411E-3	0.9	1.4
54.004	269.1	3698.1	10000	20.0	4.727	84.004	294.3	538.2	0.5468	7524	7376.2598	0.02597	14753	1.4753E6	3.411E-3	0.9	1.4
54.996	273.2	3793.7	10000	20.0	4.703	84.996	301.9	546.5	0.5524	7484	7602.0601	0.02506	15204	1.5204E6	3.411E-3	0.9	1.4
56.000	277.4	3890.2	10000	20.0	4.634	86.000	309.6	554.7	0.5581	7375	7828.9902	0.02397	15658	1.5658E6	3.411E-3	0.9	1.4
57.000	283.3	4093.6	10000	20.0	4.634	87.000	325.8	566.7	0.5749	7375	8169.3501	0.02297	16339	1.6339E6	3.411E-3	1.0	1.5
57.996	287.5	4208.8	10000	20.0	4.576	87.996	334.9	574.9	0.5825	7283	8407.8398	0.02203	16816	1.6816E6	3.411E-3	1.0	1.5
58.996	293.6	4327.6	10000	20.0	4.459	88.996	344.4	587.2	0.5865	7096	8767.1904	0.02058	17534	1.7534E6	3.411E-3	1.0	1.5
59.996	297.6	4414.7	10000	20.0	4.425	89.996	351.3	595.1	0.5903	7043	9006.7305	0.01988	18013	1.8013E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0280	300.0	4568.1	10000	20.0	4.472	92.028	363.5	600.0	0.6059	7117	290.3050	0.01977	580.61	58061	3.411E-3	0.0	1.5
1.9920	300.0	4535.6	10000	20.0	4.486	92.992	360.9	600.0	0.6015	7139	541.6510	0.01983	1083.3	1.0833E5	3.411E-3	0.0	1.5
3.0040	300.0	4516.2	10000	20.0	4.366	94.004	359.4	599.9	0.5990	6949	919.9030	0.01931	1839.8	1.8398E5	3.411E-3	0.1	1.6
4.0160	300.0	4517.0	10000	20.0	4.436	95.016	359.5	600.0	0.5991	7061	1171.3400	0.01961	2342.7	2.3427E5	3.411E-3	0.1	1.6
5.0280	300.0	4515.5	10000	20.0	4.400	96.028	359.3	600.0	0.5989	7003	1421.4200	0.01945	2842.8	2.8428E5	3.411E-3	0.1	1.6
6.0240	300.0	4518.9	10000	20.0	4.393	97.024	359.6	600.0	0.5993	6992	1800.5200	0.01942	3601.0	3.6010E5	3.411E-3	0.1	1.6
7.0160	300.0	4519.8	10000	20.0	4.400	98.016	359.7	600.0	0.5994	7003	2049.7400	0.01945	4099.5	4.0995E5	3.411E-3	0.1	1.6
8.0160	300.0	4525.9	10000	20.0	4.478	99.016	360.2	600.0	0.6003	7127	2428.8000	0.01980	4857.6	4.8576E5	3.411E-3	0.1	1.7
8.9920	300.0	4541.1	10000	20.0	4.410	99.992	361.4	600.0	0.6023	7018	2679.2400	0.01950	5358.5	5.3585E5	3.411E-3	0.1	1.7
9.9920	300.0	4523.7	10000	20.0	4.456	100.992	360.0	600.0	0.6000	7091	2929.1299	0.01970	5858.3	5.8583E5	3.411E-3	0.2	1.7
10.992	300.0	4508.2	10000	20.0	4.408	101.992	358.8	600.0	0.5979	7016	3306.2600	0.01949	6612.5	6.6125E5	3.411E-3	0.2	1.7
12.032	300.0	4554.5	10000	20.0	4.463	103.032	362.4	600.0	0.6041	7104	3559.9099	0.01973	7119.8	7.1198E5	3.412E-3	0.2	1.7
13.016	300.0	4520.9	10000	20.0	4.413	104.016	359.8	600.0	0.5996	7024	3810.9099	0.01951	7621.8	7.6218E5	3.411E-3	0.2	1.7
13.992	300.0	4485.4	10000	20.0	4.363	104.992	356.9	600.0	0.5949	6944	4186.6699	0.01929	8373.3	8.3733E5	3.411E-3	0.2	1.7
15.016	300.0	4506.7	10000	20.0	4.423	106.016	358.6	600.0	0.5977	7039	4437.2900	0.01955	8874.6	8.8746E5	3.411E-3	0.3	1.8
16.020	300.0	4520.0	10000	20.0	4.391	107.020	359.7	600.0	0.5995	6988	4814.2100	0.01941	9628.4	9.6284E5	3.411E-3	0.3	1.8
17.016	300.0	4484.7	10000	20.0	4.423	108.016	356.9	600.0	0.5948	7040	5065.4102	0.01955	10131	1.0131E6	3.411E-3	0.3	1.8
17.992	300.0	4484.6	10000	20.0	4.387	108.992	356.9	600.0	0.5948	6983	5316.9600	0.01940	10634	1.0634E6	3.411E-3	0.3	1.8
18.988	300.0	4524.2	10000	20.0	4.386	109.988	360.0	600.0	0.6000	6981	5693.9302	0.01939	11388	1.1388E6	3.411E-3	0.3	1.8
20.016	300.0	4523.2	10000	20.0	4.449	111.016	359.9	600.0	0.5999	7080	5945.1699	0.01967	11890	1.1890E6	3.411E-3	0.3	1.9
21.036	300.0	4511.9	10000	20.0	4.441	112.036	359.0	600.0	0.5985	7069	6325.1401	0.01964	12650	1.2650E6	3.411E-3	0.4	1.9
22.016	300.0	4518.5	10000	20.0	4.376	113.016	359.6	600.0	0.5993	6965	6573.5898	0.01935	13147	1.3147E6	3.411E-3	0.4	1.9
22.992	300.0	4535.7	10000	20.0	4.462	113.992	360.9	600.0	0.6016	7101	6824.8901	0.01973	13650	1.3650E6	3.411E-3	0.4	1.9
23.992	300.0	4487.9	10000	20.0	4.371	114.992	357.1	600.0	0.5952	6956	7201.7500	0.01932	14404	1.4404E6	3.411E-3	0.4	1.9
24.992	300.0	4517.6	10000	20.0	4.412	115.992	359.5	600.0	0.5992	7022	7459.7598	0.01951	14920	1.4920E6	3.411E-3	0.4	1.9
26.016	300.0	4534.4	10000	20.0	4.391	117.016	360.8	600.0	0.6014	6989	7706.4399	0.01941	15413	1.5413E6	3.411E-3	0.4	2.0
27.024	300.0	4465.5	10000	20.0	4.390	118.024	355.4	600.0	0.5922	6987	8081.6401	0.01941	16163	1.6163E6	3.411E-3	0.5	2.0
27.992	300.0	4503.1	10000	20.0	4.423	118.992	358.3	600.0	0.5973	7039	8332.7695	0.01956	16666	1.6666E6	3.411E-3	0.5	2.0
29.004	300.0	4549.0	10000	20.0	4.397	120.004	362.0	599.9	0.6034	6998	8709.7695	0.01944	17420	1.7420E6	3.411E-3	0.5	2.0
29.992	300.0	4515.6	10000	20.0	4.402	120.992	359.3	600.0	0.5989	7005	8961.0098	0.01946	17922	1.7922E6	3.411E-3	0.5	2.0
30.996	300.0	4520.8	10000	20.0	4.434	121.996	359.8	600.0	0.5996	7057	9212.5195	0.01960	18425	1.8425E6	3.411E-3	0.5	2.0
32.016	300.0	4516.4	10000	20.0	4.445	123.016	359.4	600.0	0.5990	7074	9590.7305	0.01965	19181	1.9181E6	3.411E-3	0.5	2.1
33.016	300.0	4500.0	10000	20.0	4.420	124.016	358.1	600.0	0.5968	7034	9841.6396	0.01954	19683	1.9683E6	3.411E-3	0.6	2.1
34.024	300.0	4533.9	10000	20.0	4.395	125.024	360.8	600.0	0.6014	6995	10217.800	0.01943	20436	2.0436E6	3.411E-3	0.6	2.1
34.992	300.0	4495.7	10000	20.0	4.391	125.992	357.8	600.0	0.5963	6988	10470.400	0.01941	20941	2.0941E6	3.411E-3	0.6	2.1
36.016	300.0	4489.6	10000	20.0	4.386	127.016	357.3	600.0	0.5954	6981	10722.500	0.01939	21445	2.1445E6	3.411E-3	0.6	2.1
36.992	300.0	4538.4	10000	20.0	4.457	127.992	361.2	600.0	0.6019	7093	11097.300	0.01970	22195	2.2195E6	3.411E-3	0.6	2.1
37.992	300.0	4488.0	10000	20.0	4.384	128.992	357.1	600.0	0.5952	6977	11348.800	0.01938	22698	2.2698E6	3.411E-3	0.6	2.1
38.996	300.0	4519.9	10000	20.0	4.421	129.996	359.7	600.0	0.5995	7036	11599.900	0.01955	23200	2.3200E6	3.411E-3	0.6	2.2
40.016	300.0	4527.3	10000	20.0	4.409	131.016	360.3	600.0	0.6004	7018	11978.200	0.01949	23956	2.3956E6	3.411E-3	0.7	2.2
41.016	300.0	4526.9	10000	20.0	4.409	132.016	360.2	600.0	0.6004	7018	12228.300	0.01949	24457	2.4457E6	3.411E-3	0.7	2.2
42.016	300.0	4491.2	10000	20.0	4.390	133.016	357.4	600.0	0.5957	6986	12605.400	0.01941	25211	2.5211E6	3.411E-3	0.7	2.2
43.016	300.0	4494.5	10000	20.0	4.366	134.016	357.7	600.0	0.5961	6949	12857.900	0.01930	25716	2.5716E6	3.411E-3	0.7	2.2
44.016	300.0	4458.9	10000	20.0	4.363	135.016	354.8	600.0	0.5914	6944	13108.000	0.01929	26216	2.6216E6	3.411E-3	0.7	2.3
45.016	300.0	4511.4	10000	20.0	4.416	136.016	359.0	600.0	0.5983	7028	13487.300	0.01952	26975	2.6975E6	3.411E-3	0.8	2.3
46.016	300.0	4545.0	10000	20.0	4.401	137.016	361.7	600.0	0.6028	7004	13736.500	0.01946	27473	2.7473E6	3.411E-3	0.8	2.3
47.032	300.0	4522.7	10000	20.0	4.372	138.032	359.9	600.0	0.5998	6958	14113.200	0.01933	28226	2.8226E6	3.411E-3	0.8	2.3
47.992	300.0	4483.9	10000	20.0	4.419	138.992	356.8	600.1	0.5946	7033	14364.700	0.01953	28729	2.8729E6	3.411E-3	0.8	2.3
49.016	300.0	4492.5	10000	20.0	4.391	140.016	357.5	600.0	0.5958	6988	14617.200	0.01941	29234	2.9234E6	3.411E-3	0.8	2.3
50.016	300.0	4515.4	10000	20.0	4.427	141.016	359.3	600.0	0.5989	7046	14993.000	0.01957	29986	2.9986E6	3.411E-3	0.8	2.4
51.028	300.0	4512.8	10000	20.0	4.375	142.028	359.1	600.0	0.5986	6963	15244.300	0.01934	30489	3.0489E6	3.411E-3	0.9	2.4
52.024	300.0	4490.2	10000	20.0	4.396	143.024	357.3	600.0	0.5955	6996	15622.600	0.01943	31245	3.1245E6	3.411E-3	0.9	2.4
52.992	300.0	4508.8	10000	20.0	4.377	143.992	358.8	600.0	0.5980	6966	15872.700	0.01935	31745	3.1745E6	3.411E-3	0.9	2.4
53.992	300.0	4515.7	10000	20.0	4.421	144.992	359.4	600.0	0.5989	7036	16123.900	0.01954	32248	3.2248E6	3.411E-3	0.9	2.4
54.988	300.0	4480.7	10000	20.0	4.354	145.988	356.6	600.0	0.5943	6930	16501.000	0.01925	33002	3.3002E6	3.411E-3	0.9	2.4
56.016	300.0	4546.5	10000	20.0	4.467	147.016	361.8	600.0	0.6030	7110	16752.301	0.01975	33505	3.3505E6	3.412E-3	0.9	2.5
57.016	300.0	4528.3	10000	20.0	4.423	148.016	360.3	600.0	0.6006	7039	17133.199	0.01955	34266	3.4266E6	3.411E-3	1.0	2.5
57.992	300.0	4515.7	10000	20.0	4.418	148.992	359.3	600.0	0.5989	7031	17380.600	0.01953	34761	3.4761E6	3.411E-3	1.0	2.5
59.004	300.0	4482.3	10000	20.0	4.379	150.004	356.7	600.0	0.5945	6969	17635.100	0.01936	35270	3.5270E6	3.411E-3	1.0	2.5
60.016	300.0	4529.6	10000	20.0	4.388	151.016	360.5	600.0	0.6008	6983	18008.801	0.01940	36018	3.6018E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	297.5	4458.3	10000	20.0	4.471	152.004	354.8	595.0	0.5962	7116	226.8050	0.02010	453.61	45361	3.411E-3	0.0	2.5
2.0080	291.5	4280.5	10000	20.0	4.471	153.008	340.6	583.1	0.5842	7116	585.2590	0.02093	1170.5	1.1705E5	3.411E-3	0.0	2.6
3.0040	287.5	4210.2	10000	20.0	4.565	154.004	335.0	574.9	0.5828	7266	822.1500	0.02198	1644.3	1.6443E5	3.411E-3	0.1	2.6
4.0040	281.3	3981.2	10000	20.0	4.614	155.004	316.8	562.6	0.5631	7344	1172.7300	0.02320	2345.5	2.3455E5	3.411E-3	0.1	2.6
5.0040	277.3	3895.8	10000	20.0	4.658	156.004	310.0	554.6	0.5590	7413	1397.9399	0.02410	2795.9	2.7959E5	3.411E-3	0.1	2.6
6.0040	273.2	3770.5	10000	20.0	4.669	157.004	300.0	546.5	0.5490	7430	1623.4800	0.02488	3247.0	3.2470E5	3.411E-3	0.1	2.6
7.0040	267.1	3635.3	10000	20.0	4.764	158.004	289.3	534.1	0.5416	7582	1962.7900	0.02658	3925.6	3.9256E5	3.411E-3	0.1	2.6
8.0040	263.0	3500.6	10000	20.0	4.790	159.004	278.6	526.0	0.5295	7624	2174.3501	0.02755	4348.7	4.3487E5	3.411E-3	0.1	2.7
9.0040	256.9	3330.1	10000	20.0	4.829	160.004	265.0	513.9	0.5157	7686	2493.6299	0.02911	4987.3	4.9873E5	3.411E-3	0.2	2.7
10.004	252.8	3271.6	10000	20.0	4.851	161.004	260.3	505.6	0.5149	7720	2706.4500	0.03020	5412.9	5.4129E5	3.411E-3	0.2	2.7
11.004	246.7	3135.0	10000	20.0	4.903	162.004	249.5	493.3	0.5057	7803	3014.1101	0.03206	6028.2	6.0282E5	3.411E-3	0.2	2.7
12.004	242.6	3010.0	10000	20.0	4.933	163.004	239.5	485.2	0.4937	7852	3214.2500	0.03336	6428.5	6.4285E5	3.411E-3	0.2	2.7
13.000	238.5	2898.3	10000	20.0	4.978	164.000	230.6	477.0	0.4835	7922	3413.6899	0.03482	6827.4	6.8274E5	3.411E-3	0.2	2.7
14.004	232.4	2764.8	10000	20.0	5.034	165.004	220.0	464.7	0.4734	8012	3701.5100	0.03710	7403.0	7.4030E5	3.411E-3	0.2	2.8
15.004	228.3	2702.4	10000	20.0	5.083	166.004	215.1	456.7	0.4709	8089	3889.3000	0.03879	7778.6	7.7786E5	3.411E-3	0.3	2.8
16.000	222.1	2563.5	10000	20.0	5.104	167.000	204.0	444.3	0.4592	8123	4170.8301	0.04115	8341.7	8.3417E5	3.411E-3	0.3	2.8
17.004	218.0	2456.0	10000	20.0	5.150	168.004	195.4	436.0	0.4482	8196	4352.2100	0.04311	8704.4	8.7044E5	3.412E-3	0.3	2.8
18.012	211.9	2335.6	10000	20.0	5.218	169.012	185.9	423.8	0.4385	8305	4617.5000	0.04623	9235.0	9.2350E5	3.412E-3	0.3	2.8
19.004	207.8	2259.2	10000	20.0	5.209	170.004	179.8	415.6	0.4326	8290	4789.8999	0.04799	9579.8	9.5798E5	3.411E-3	0.3	2.8
20.004	203.6	2161.0	10000	20.0	5.236	171.004	172.0	407.2	0.4223	8333	4965.7798	0.05026	9931.6	9.9316E5	3.411E-3	0.3	2.9
21.004	197.5	2059.6	10000	20.0	5.294	172.004	163.9	395.0	0.4150	8426	5208.8999	0.05401	10418	1.0418E6	3.411E-3	0.4	2.9
22.008	193.4	1951.9	10000	20.0	5.301	173.008	155.3	386.8	0.4016	8437	5373.9102	0.05640	10748	1.0748E6	3.411E-3	0.4	2.9
23.004	187.1	1848.7	10000	20.0	5.376	174.004	147.1	374.2	0.3931	8556	5611.4902	0.06109	11223	1.1223E6	3.411E-3	0.4	2.9
24.004	183.1	1770.2	10000	20.0	5.387	175.004	140.9	366.2	0.3847	8573	5759.0801	0.06392	11518	1.1518E6	3.411E-3	0.4	2.9
25.004	179.0	1684.4	10000	20.0	5.416	176.004	134.0	358.0	0.3744	8619	5909.7998	0.06726	11820	1.1820E6	3.411E-3	0.4	2.9
26.004	172.6	1586.7	10000	20.0	5.453	177.004	126.3	345.3	0.3657	8678	6134.0698	0.07279	12268	1.2268E6	3.411E-3	0.4	3.0
27.004	168.6	1508.7	10000	20.0	5.470	178.004	120.1	337.2	0.3561	8705	6273.7002	0.07657	12547	1.2547E6	3.411E-3	0.5	3.0
28.004	162.4	1400.1	10000	20.0	5.503	179.004	111.4	324.8	0.3430	8758	6478.3301	0.08300	12957	1.2957E6	3.411E-3	0.5	3.0
29.004	158.2	1341.7	10000	20.0	5.528	180.004	106.8	316.3	0.3375	8799	6615.1802	0.08793	13230	1.3230E6	3.411E-3	0.5	3.0
30.004	154.1	1257.6	10000	20.0	5.555	181.004	100.1	308.3	0.3247	8841	6739.9302	0.09304	13480	1.3480E6	3.411E-3	0.5	3.0
31.008	148.0	1169.8	10000	20.0	5.583	182.008	93.09	296.0	0.3145	8885	6927.2402	0.1014	13854	1.3854E6	3.411E-3	0.5	3.0
32.004	143.7	1104.7	10000	20.0	5.601	183.004	87.91	287.5	0.3058	8914	7055.5698	0.1079	14111	1.4111E6	3.411E-3	0.5	3.1
33.004	139.5	1037.6	10000	20.0	5.615	184.004	82.57	279.0	0.2960	8936	7171.2300	0.1148	14342	1.4342E6	3.411E-3	0.6	3.1
34.004	133.4	955.23	10000	20.0	5.648	185.004	76.01	266.8	0.2850	8989	7339.1602	0.1263	14678	1.4678E6	3.411E-3	0.6	3.1
35.004	129.1	899.41	10000	20.0	5.676	186.004	71.57	258.3	0.2771	9033	7451.3501	0.1354	14903	1.4903E6	3.411E-3	0.6	3.1
36.004	124.8	833.64	10000	20.0	5.681	187.004	66.34	249.5	0.2659	9042	7563.5298	0.1452	15127	1.5127E6	3.411E-3	0.6	3.1
37.000	118.5	748.97	10000	20.0	5.700	188.000	59.60	237.1	0.2514	9072	7713.1499	0.1614	15426	1.5426E6	3.412E-3	0.6	3.1
38.004	114.3	704.70	10000	20.0	5.720	189.004	56.08	228.6	0.2453	9103	7812.7300	0.1742	15625	1.5625E6	3.411E-3	0.6	3.2
39.004	109.9	653.86	10000	20.0	5.740	190.004	52.03	219.8	0.2367	9135	7913.6602	0.1891	15827	1.5827E6	3.411E-3	0.7	3.2
40.004	103.7	575.53	10000	20.0	5.757	191.004	45.80	207.4	0.2208	9162	8043.7998	0.2130	16088	1.6088E6	3.411E-3	0.7	3.2
41.012	99.45	531.33	10000	20.0	5.771	192.012	42.28	198.9	0.2126	9186	8132.7998	0.2322	16266	1.6266E6	3.411E-3	0.7	3.2
42.000	95.01	486.14	10000	20.0	5.777	193.000	38.69	190.0	0.2036	9195	8217.2998	0.2546	16435	1.6435E6	3.411E-3	0.7	3.2
43.004	88.82	427.26	10000	20.0	5.798	194.004	34.00	177.6	0.1914	9228	8329.7900	0.2924	16660	1.6660E6	3.411E-3	0.7	3.2
44.004	84.57	385.16	10000	20.0	5.805	195.004	30.65	169.1	0.1812	9238	8403.7197	0.3229	16807	1.6807E6	3.411E-3	0.7	3.3
45.004	80.09	353.03	10000	20.0	5.811	196.004	28.09	160.2	0.1754	9249	8478.1699	0.3605	16956	1.6956E6	3.411E-3	0.8	3.3
46.004	73.49	304.58	10000	20.0	5.825	197.004	24.24	147.0	0.1649	9271	8577.3301	0.4292	17155	1.7155E6	3.411E-3	0.8	3.3
47.004	69.19	274.70	10000	20.0	5.836	198.004	21.86	138.4	0.1580	9288	8639.2402	0.4850	17278	1.7278E6	3.411E-3	0.8	3.3
48.004	64.61	238.66	10000	20.0	5.841	199.004	18.99	129.2	0.1470	9296	8701.0596	0.5567	17402	1.7402E6	3.411E-3	0.8	3.3
49.004	59.95	213.65	10000	20.0	5.848	200.004	17.00	119.9	0.1418	9307	8756.5498	0.6474	17513	1.7513E6	3.411E-3	0.8	3.3
50.004	55.72	188.66	10000	20.0	5.855	201.004	15.01	111.4	0.1347	9319	8831.2998	0.7504	17663	1.7663E6	3.411E-3	0.8	3.4
51.004	51.15	162.89	10000	20.0	5.864	202.004	12.96	102.3	0.1267	9333	8880.2402	0.8918	17760	1.7760E6	3.411E-3	0.9	3.4
52.004	43.79	121.44	10000	20.0	5.867	203.004	9.664	87.57	0.1104	9338	8922.7305	1.218	17845	1.7845E6	3.411E-3	0.9	3.4
53.004	39.41	100.88	10000	20.0	5.870	204.004	8.028	78.81	0.1019	9343	8959.4502	1.504	17919	1.7919E6	3.411E-3	0.9	3.4
54.004	34.50	82.365	10000	20.0	5.874	205.004	6.554	69.00	0.09499	9348	8996.0996	1.963	17992	1.7992E6	3.411E-3	0.9	3.4
55.004	29.34	61.727	10000	20.0	5.878	206.004	4.912	58.69	0.08370	9355	9026.1504	2.716	18052	1.8052E6	3.411E-3	0.9	3.4
56.004	24.92	47.393	10000	20.0	5.879	207.004	3.771	49.83	0.07568	9357	9050.2500	3.768	18101	1.8101E6	3.411E-3	0.9	3.5
57.004	19.61	30.993	10000	20.0	5.883	208.004	2.466	39.22	0.06288	9363	9073.8701	6.086	18148	1.8148E6	3.411E-3	1.0	3.5
58.004	16.41	23.022	10000	20.0	5.884	209.004	1.832	32.82	0.05583	9365	9085.2500	8.696	18171	1.8171E6	3.411E-3	1.0	3.5
59.004	11.31	11.997	10000	20.0	5.891	210.004	0.9547	22.62	0.04221	9376	9096.9004	18.32	18194	1.8194E6	3.411E-3	1.0	3.5
60.004	5.788	2.8014	10000	20.0	5.891	211.004	0.2229	11.58	0.01926	9376	9104.7803	69.97	18210	1.8210E6	3.411E-3	1.0	3.5

